MetaChrom

Device for testing friction and abrasion of catalysts "PTI-1"

RPC “META-CHROM”, Co. Ltd presents a multifunctional device “PTI-1”, which allows to determine the resistance of granular catalysts and adsorbents to friction and abrasion according to SPENCE and ASTM D4058 standardss

With an installed drum nozzle (a).
On the right is a cylindrical nozzle (b).

Figure 1 – Device for testing friction and abrasion of catalysts “PTI-1” with an installed drum nozzle (a). On the right is a cylindrical nozzle (b).

Application of the device "PTI-1" for testing a granular sample for friction / abrasion (drum nozzle, ASTM D4058 -96 method).

The granulated sample (catalyst, catalyst carrier, adsorbent) is loaded into the drum nozzle. The drum nozzle makes 60 rpm for 30 minutes. At the end of the process, the tested sample is separated from the dust by sieving through a sieve (ASTM N°20 mesh 0.85 mm). By weighing the original sample and the residue on the sieve, the attrition loss of the granular sample is determined.

Calculation: Abrasion loss % = M1-M2/M1*100

where

М1 – is the mass of a fresh sample after sieving;

М2 – is the mass of the tested sample after sieving.

Application of the device "PTI-1" for testing a granular sample for abrasion (cylindrical nozzle, SPENCE method).

Granular sample from 1 to 4 pieces, 25 grams each, is loaded into four cylinders. The cylindrical nozzle makes 25 rpm for 60 minutes. At the end of the process, the contents of the cylinders are sifted through a sieve (the mesh size is 2/3 of the smallest granule size). The initial sample, the sifted sample, and the remaining fines (“dust”) are weighed. Based on the measured masses, the abrasion loss and abrasion resistance are calculated. This method has a wider particle size range than the ASTM method.

Calculationformulas: Abrasion loss % = M3/M1*100

Abrasion resistance % = M2/M1*100

where

М1 – initial mass of a fresh sample after sieving;

М2 – mass of the tested sample after sieving;

М3 – mass of dust.

Device advantages

The device “PTI-1” performs smooth acceleration and deceleration of the nozzle in order to avoid the effects of shock loads on the test sample, has the flexibility to set the parameters of the test process, thanks to the ability to set custom nozzle rotation speeds, test duration (from 1 min. to 7 days) and direction rotation regardless of the nozzle used, with the ability to save modes.

The device is run by a controller, all settings are made using the buttons on the front panel. Information is displayed with an intuitive user interface.

The design of the device provides three fixed positions of the nozzle for quick loading, testing and unloading of the test sample.The device has low consumption (up to 18 W) and low weight (12.5 kg). The use of a stepper motor with a gearbox provides a small error in maintaining speed (± 0.3 rpm).

Device advantages

Basic operatingmodes:

· Preset rotating drum method (ASTM D4058 -96) (60 rpm, 30 min).

· Preset rotating cylinder method (SPENCE) (25 rpm, 60 min).

· User mode with arbitrary setting of rotation frequency (from 10 to 60 rpm) and test duration (from 1 minute to 7 days).

Electricmotor

Steppermotorwithgearbox

Speed maintenanceerror, rpm:

± 0,3

Control

Digital (controller)

Power supply:

100-240 V,  50/60Hz

Power consumption:

18 W

Allowedsampleweight:

Notmorethan 100 g.

Mass:

12.5 kg with cylindrical nozzle

10.8 kg with drum head

Overalldimensions, cm:

 

withcylindricalnozzle

38,9х31,4х45,9

withdrumattachment

48,5х30,4х45,4

Sievemeshsizes, mm:

 

by ASTM method

ASTM No20  0.85

according to the SPENCE method

2/3 of the minimum granule size. At the request of the customer.

Scales (at the request of the customer)

 

Operatingconditions

UHL 4.2

Ambienttemperature

from 10 °С to 35 °С

Relative air humidity at 25˚С, %

no more than 80%

Atmospherepressure

84 to 107 kPa (630 to 800 mmHg)

Contents of delivery

Designationa

Q-ty, pcs.

Device PTI-1

1

Drumnozzle

1

Cylindernozzle

1

Screen according to ASTM D4058 (ASTM N°20 mesh 0.85mm)

1

Sieve according to the SPENCE method (according to the customer’s request)

1

4 hexnozzlefixingscrew

2

Hex Key 4

1

Power cord

1

Passport

1

Manual

1

Scales (at the request of the customer)

1

ContactS

QUALITY MARK «ANALYTICAL CHEMISTRY»

CUSTOMS UNION DECLARATION OF CONFORMITY CRYSTALLUX

QUALITY MARK «MEASURING INSTRUMENT»

CERTIFICATE OF CONFORMITY GOST R ISO 9001

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